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Synthesis

SiliCycle offers silica-based products that can be used in organic synthesis in replacement of homogeneous equivalents. In many cases, supported reagents have distinct advantages over their solution-phase counterparts, the biggest one being the ability to do multiple transformations in a single pot, the immobilization of toxic reagents, and increased selectivity. They are also suitable for use in batch reactions and in flow through applications.

Application Notes

All available applications developed for synthesis purposes are listed below:

General applications

  • Common Organic Reactions

For amide and ester synthesis refer to the following link for more information

Other applications

  • Use of SiliaBond Cyanoborohydride
  • Use of SiliaBond Carbonate
  • Difference Between SiliaBond PCC & PDC: When to Use Them?

SiliaBond Kit 

  • SiliaBond Reagents Kit for Microwave Applications

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  1. SiliaPrep™ 96 Well Plates Carbonate

    SiliaPrep™ 96 Well Plates Carbonate


    Standard SiliaPrep 96 Well Plates are available in 2 mL with different bed weight up to 200 mg. Various sorbents are available and are divided into several sections based on sorbent characteristics.
  2. SiliaSep™ Flash Cartridges - Büchi™ Compatible (BU) Amine

    SiliaSep™ Flash Cartridges - Büchi™ Compatible (BU) Amine

    SiliaSep™ BU flash cartridges are compatible with Büchi Sepacor flash chromatography instrument.

    Good alternative for normal phase purification of compounds with basic properties, which would normally have to be purified by reversed-phase.

  3. SiliaSep™ Flash Cartridges - Biotage™ Compatible (BT) Amine

    SiliaSep™ Flash Cartridges - Biotage™ Compatible (BT) Amine

    SiliaSep™ BT flash cartridges are compatible with Biotage i-style compression modules.

    Good alternative for normal phase purification of compounds with basic properties, which would normally have to be purified by reversed-phase.

  4. SiliaSep™ Flash Cartridges - Open Top (OT) TMA Acetate nec

    SiliaSep™ Flash Cartridges - Open Top (OT) TMA Acetate nec

    SiliaSep™ OT flash cartridges are compatible with FlashMaster instrument.

    Packed with a strong anion exchanger, they can be used to fully retain acidic compounds for clean-up or to isolate them by “Catch and Release” process.

  5. SiliaSep™ Flash Cartridges TMA Acetate nec

    SiliaSep™ Flash Cartridges TMA Acetate nec

    Packed with a strong anion exchanger, they can be used to fully retain acidic compounds for clean-up or to isolate them by catch and release process.

    SiliaSep flash TMA Acetate cartridges offer a superior alternative to the other cartridges available on the market.

  6. SiliaSep™ Flash Cartridges TMA Chloride (SAX)

    SiliaSep™ Flash Cartridges TMA Chloride (SAX)

    Packed with a strong anion exchanger, they can be used to fully retain acidic compounds for clean-up or to isolate them by catch and release process.

    SiliaSep flash TMA Chloride cartridges offer a superior alternative to the other cartridges available on the market.

  7. SiliaSep™ Flash Cartridges - Open Top (OT) Amine

    SiliaSep™ Flash Cartridges - Open Top (OT) Amine

    SiliaSep™ OT flash cartridges are compatible with FlashMaster instrument.

    Good alternative for normal phase purification of compounds with basic properties, which would normally have to be purified by reversed-phase.

  8. SiliaSep™ Flash Cartridges Amine

    SiliaSep™ Flash Cartridges Amine

    Good alternative for normal phase purification of compounds with basic properties, which would normally have to be purified by reversed-phase.

    SiliaSep flash amine cartridges offer a superior alternative to the other cartridges available on the market.

  9. SiliaPrep™ SPE Cartridges TMA Chloride nec (SAX)

    SiliaPrep™ SPE Cartridges TMA Chloride nec (SAX)

    SiliaPrep TMA Chloride (SAX) is a strong anion exchanger sorbent positively charged under all conditions used to extract acid molecules (pKa 3-5).

  10. SiliaMetS® TAAcONa

    SiliaMetS® TAAcONa

    SiliaMetS® TAAcONa or (or SiliaMetS Triaminetetraacetate, sodium salt) is a silica bound metal scavenger for Pd(II), Ni(II) and Cu. It is the supported version of EDTA in its sodium salt form. It is an effective scavenger for metals in higher oxidation state, 2+ or higher.

  11. SiliaPlate™ TLC Plates - Aluminum (Al) Silica

    SiliaPlate™ TLC Plates - Aluminum (Al) Silica

    Standard normal phase Analytical SiliaPlate™ made with SiliaFlash® silica gel are available on aluminum backing. Different sizes available.

  12. SiliaPlate™ TLC Plates - Glass (G) Diol

    SiliaPlate™ TLC Plates - Glass (G) Diol

    Analytical SiliaPlate™ made with diol-functionalized silica gel are available on glass backing.

  13. SiliaPlate™ TLC Plates - Glass (G) CN

    SiliaPlate™ TLC Plates - Glass (G) CN

    Analytical SiliaPlate™ made with cyano-functionalized silica gel are available on glass backing.

  14. SiliaPlate™ TLC Plates - Glass (G) NH2

    SiliaPlate™ TLC Plates - Glass (G) NH2

    Analytical SiliaPlate™ made with amino-functionalized silica gel are available on glass backing.

  15. SiliaPlate™ TLC Plates - Glass (G) C2

    SiliaPlate™ TLC Plates - Glass (G) C2

    Standard reverse-phase Analytical SiliaPlate™ made with C2 silica gel are available on glass backing.

  16. SiliaPlate™ TLC Plates - Glass (G) C8

    SiliaPlate™ TLC Plates - Glass (G) C8

    Standard reverse-phase Analytical SiliaPlate™ made with C8 silica gel are available on glass backing.

  17. SiliaPlate™ TLC Plates - Glass (G - Scored) Silica

    SiliaPlate™ TLC Plates - Glass (G - Scored) Silica

    Standard normal phase Analytical SiliaPlate™ made with SiliaFlash® silica gel are available on scored glass backing. Different sizes available.

  18. SiliaPlate™ TLC Plates - Glass (G) Silver Nitrate (AgNO3) nec

    SiliaPlate™ TLC Plates - Glass (G) Silver Nitrate (AgNO3) nec

    Analytical SiliaPlate™ made with silver nitrate impregnated silica gel are available on glass backing. 

  19. SiliaPlate™ TLC Plates - Glass (G) C18

    SiliaPlate™ TLC Plates - Glass (G) C18

    Standard reverse-phase Analytical SiliaPlate™ made with C18 silica gel are available on glass backing.

  20. SiliaPlate™ TLC Plates - Glass (G - Preparative) Silica

    SiliaPlate™ TLC Plates - Glass (G - Preparative) Silica

    Phase Preparative SiliaPlate™ made with silica gel are available on glass backing.

  21. SiliaSep™ Flash Cartridges - Büchi™ Compatible (BU) SCX

    SiliaSep™ Flash Cartridges - Büchi™ Compatible (BU) SCX

    SiliaSep™ BU flash cartridges are compatible with Büchi Sepacor flash chromatography instrument.

    Packed with a strong cation exchanger, they can be used to fully retain basic compounds for clean-up or to isolate them by catch and release process.

  22. SiliaSep™ Flash Cartridges - Biotage™ Compatible (BT) Propylsulfonic Acid (SCX-2)

    SiliaSep™ Flash Cartridges - Biotage™ Compatible (BT) Propylsulfonic Acid (SCX-2)

    SiliaSep™ BT flash cartridges are compatible with Biotage i-style compression modules.

    Packed with a strong cation exchanger (SiliaBond® Propylsulfonic Acid), they can be used to fully retain basic compounds for clean-up or to isolate them by “Catch and Release” process.

  23. SiliaSep™ Flash Cartridges - Open Top (OT) Thiol

    SiliaSep™ Flash Cartridges - Open Top (OT) Thiol

    SiliaSep™ OT flash cartridges are compatible with FlashMaster instrument.

  24. SiliaSep™ Flash Cartridges - Open Top (OT) Carbonate

    SiliaSep™ Flash Cartridges - Open Top (OT) Carbonate

    SiliaSep™ OT flash cartridges are compatible with FlashMaster instrument.

  25. SiliaSep™ Flash Cartridges - Open Top (OT) Tosic Acid (SCX)

    SiliaSep™ Flash Cartridges - Open Top (OT) Tosic Acid (SCX)

    SiliaSep™ OT flash cartridges are compatible with FlashMaster instrument.

    Packed with a strong cation exchanger, they can be used to fully retain basic compounds for clean-up or to isolate them by “Catch and Release” process.

  26. SiliaSep™ Flash Cartridges - Open Top (OT) Propylsulfonic Acid (SCX-2)

    SiliaSep™ Flash Cartridges - Open Top (OT) Propylsulfonic Acid (SCX-2)

    SiliaSep™ OT flash cartridges are compatible with FlashMaster instrument.

    Packed with a strong cation exchanger (SiliaBond® Propylsulfonic Acid), they can be used to fully retain basic compounds for clean-up or to isolate them by “Catch and Release” process.

  27. SiliaSep™ Flash Cartridges Cysteine

    SiliaSep™ Flash Cartridges Cysteine

    SiliaSep flash cysteine cartridges offer a superior alternative to the other cartridges available on the market .

  28. SiliaSep™ Flash Cartridges Dimercaptotriazine (DMT)

    SiliaSep™ Flash Cartridges Dimercaptotriazine (DMT)

    SiliaSep flash DMT cartridges offer a superior alternative to the other cartridges available on the market.

  29. SiliaSep™ Flash Cartridges Thiourea

    SiliaSep™ Flash Cartridges Thiourea

    SiliaSep flash thiourea cartridges offer a superior alternative to the other cartridges available on the market.

  30. SiliaSep™ Flash Cartridges TAAcONa

    SiliaSep™ Flash Cartridges TAAcONa

    SiliaSep flash TAAcONa cartridges offer a superior alternative to the other cartridges available on the market.

  31. SiliaSep™ Flash Cartridges TAAcOH

    SiliaSep™ Flash Cartridges TAAcOH

    SiliaSep flash TAAcOH cartridges offer a superior alternative to the other cartridges available on the market.

  32. SiliaSep™ Flash Cartridges Thiol

    SiliaSep™ Flash Cartridges Thiol

    SiliaSep flash thiol cartridges offer a superior alternative to the other cartridges available on the market.

  33. SiliaSep™ Flash Cartridges Diamine

    SiliaSep™ Flash Cartridges Diamine

    SiliaSep flash diamine cartridges offer a superior alternative to the other cartridges available on the market.

  34. SiliaSep™ Flash Cartridges Triamine

    SiliaSep™ Flash Cartridges Triamine

    SiliaSep flash triamine cartridges offer a superior alternative to the other cartridges available on the market.

  35. SiliaSep™ Flash Cartridges Propylsulfonic Acid (SCX-2)

    SiliaSep™ Flash Cartridges Propylsulfonic Acid (SCX-2)

    Packed with a strong cation exchanger (SiliaBond® Propylsulfonic Acid), they can be used to fully retain basic compounds for clean-up or to isolate them by catch and release process.

    SiliaSep flash propylsulfonic acid cartridges offer a superior alternative to the other cartridges available on the market..

  36. SiliaSep™ Flash Cartridges Tosic Acid (SCX)

    SiliaSep™ Flash Cartridges Tosic Acid (SCX)

    Packed with a strong cation exchanger, they can be used to fully retain basic compounds for clean-up or to isolate them by catch and release process.

    SiliaSep flash propylsulfonic acid cartridges offer a superior alternative to the other cartridges available on the market.

  37. SiliaPlate™ TLC Plates - Glass (G) Silica

    SiliaPlate™ TLC Plates - Glass (G) Silica

    Standard normal phase Analytical SiliaPlate™ made with SiliaFlash® silica gel are available on glass backing. Different sizes available.

  38. SiliaCat® Heterogeneous Catalysts TEMPO

    SiliaCat® Heterogeneous Catalysts TEMPO

    SiliaCat® TEMPO is a heterogeneous catalyst/reagent made from a proprietary class of organosilica-entrapped radicals suitable for the selective oxidation of delicate substrates into valued carbonyl derivatives.

  39. SiliaCat® Heterogeneous Catalysts S-Pd

    SiliaCat® Heterogeneous Catalysts S-Pd

    The significant costs associated with precious metal catalysts and their undesired tendency to remain in organic products has generated interest for an increase in reactivity and ways to recover and reuse these metals. SiliaCat® S-Pd is a unique thiol based palladium (II) heterogeneous catalysts made from a leach-resistant organoceramic matrix.

  40. SiliaCat® Heterogeneous Catalysts DPP-Pd

    SiliaCat® Heterogeneous Catalysts DPP-Pd

    The significant costs associated with precious metal catalysts and their undesired tendency to remain in organic products has generated interest for an increase in reactivity and ways to recover and reuse these metals. SiliaCat® DPP-Pd is a unique diphenylphosphine palladium (II) heterogeneous catalysts made from a leach-resistant organoceramic matrix.

  41. SiliaPrep™ SPE Cartridges Dimercaptotriazine (DMT)

    SiliaPrep™ SPE Cartridges Dimercaptotriazine (DMT)

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  42. SiliaPrep™ SPE Cartridges TAAcONa

    SiliaPrep™ SPE Cartridges TAAcONa

    SiliaPrep Metal Scavengers will lower the residual metal concentration of variois metal complexes to single digit ppm.

  43. SiliaPrep™ SPE Cartridges TAAcOH

    SiliaPrep™ SPE Cartridges TAAcOH

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  44. SiliaPrep™ SPE Cartridges Thiourea

    SiliaPrep™ SPE Cartridges Thiourea

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  45. SiliaPrep™ SPE Cartridges Thiol

    SiliaPrep™ SPE Cartridges Thiol

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  46. SiliaPrep™ SPE Cartridges Triamine

    SiliaPrep™ SPE Cartridges Triamine

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  47. SiliaPrep™ SPE Cartridges Diamine nec

    SiliaPrep™ SPE Cartridges Diamine nec

    SiliaPrep diamine can be used in replacement of SAX for strong anions to be irreversible retention. Can also be employed as metal scavenger and in normal-phase conditions.

  48. SiliaPrep™ SPE Cartridges Diamine

    SiliaPrep™ SPE Cartridges Diamine

    SiliaPrep diamine can be used in replacement of SAX for strong anions to be irreversible retention. Can also be employed as metal scavenger and in normal-phase conditions.

  49. SiliaPrep™ SPE Cartridges Dichlorotriazine (DCT)

    SiliaPrep™ SPE Cartridges Dichlorotriazine (DCT)

    SiliaPrep Dichlorotriazine has been designed as a reagent for amide coupling applications.

  50. SiliaPrep™ SPE Cartridges Carbodiimide (DCC)

    SiliaPrep™ SPE Cartridges Carbodiimide (DCC)

    SiliaPrep Dichlorotriazine has been designed as a reagent for amide coupling applications.

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Filter By
Metal to Remove
Silver (Ag)
  1. Preferred Scavengers (4)
  2. Scavenge (3)
Calcium (Ca)
  1. Preferred Scavengers (3)
  2. Scavenge (2)
Cadmium (Cd)
  1. Preferred Scavengers (13)
  2. Scavenge (7)
Cobalt (Co)
  1. Preferred Scavengers (4)
  2. Scavenge (17)
Chromium (Cr)
  1. Preferred Scavengers (14)
  2. Scavenge (9)
Cesium (Cs)
  1. Preferred Scavengers (3)
  2. Scavenge (5)
Copper (Cu)
  1. Preferred Scavengers (4)
  2. Scavenge (26)
Iron (Fe)
  1. Preferred Scavengers (6)
  2. Scavenge (23)
Mercury (Hg)
  1. Preferred Scavengers (4)
  2. Scavenge (11)
Iridium (Ir)
  1. Preferred Scavengers (8)
  2. Scavenge (4)
Lanthanum (La)
  1. Preferred Scavengers (3)
  2. Scavenge (2)
Lithium (Li)
  1. Preferred Scavengers (3)
Magnesium (Mg)
  1. Preferred Scavengers (3)
  2. Scavenge (2)
Nickel (Ni)
  1. Preferred Scavengers (9)
  2. Scavenge (8)
Osmium (Os)
  1. Preferred Scavengers (15)
  2. Scavenge (4)
Lead (Pb)
  1. Preferred Scavengers (3)
  2. Scavenge (15)
Palladium (Pd-2+)
  1. Preferred Scavengers (17)
  2. Scavenge (16)
Palladium (Pd-0)
  1. Preferred Scavengers (17)
  2. Scavenge (9)
Platinum (Pt)
  1. Preferred Scavengers (17)
  2. Scavenge (2)
Rhodium (Rh-1+)
  1. Preferred Scavengers (10)
  2. Scavenge (16)
Rhodium (Rh-2+)
  1. Preferred Scavengers (10)
  2. Scavenge (16)
Rhodium (Rh-3+)
  1. Preferred Scavengers (6)
  2. Scavenge (7)
Ruthenium (Ru-2+)
  1. Preferred Scavengers (5)
  2. Scavenge (14)
Scandium (Sc)
  1. Preferred Scavengers (8)
  2. Scavenge (10)
Tin (Sn)
  1. Preferred Scavengers (5)
  2. Scavenge (10)
Tungsten (W)
  1. Preferred Scavengers (2)
  2. Scavenge (13)
Zinc (Zn)
  1. Preferred Scavengers (1)
  2. Scavenge (22)
Scavenge Others
  1. Scavenge (1)
Family / Formats
  1. SiliaBond® (Functionalized Silicas) (45)
  2. SiliaCat® (Heterogeneous Catalysts) (3)
  3. SiliaMetS® (Metal Scavengers) (8)
  4. SiliaPlate™ (TLC Plates) (10)
  5. SiliaSep™ (Flash Cartridges) (23)
  6. SiliaPrep™ (SPE Cartridges) (24)
Phases
  1. Aluminum Chloride (1)
  2. Amine (10)
  3. BTMA Chloride (1)
  4. C18 (1)
  5. C2 (1)
  6. C8 (1)
  7. Carbodiimide (DCC) (3)
  8. Carbonate (5)
  9. Carboxylic Acid (WCX) (4)
  10. CN (1)
  11. Cyanoborohydride (2)
  12. Cysteine (3)
  13. Diamine (5)
  14. Dichlorotriazine (DCT) (3)
  15. Diethylamine (2)
  16. Diethylamine (WAX-2) (1)
  17. Dimercaptotriazine (DMT) (4)
  18. Dimethylamine (2)
  19. Diol (1)
  20. Diphenylphosphine (1)
  21. DMAP (3)
  22. DPP-Pd (1)
  23. Ethyl Carbodiimide (EDC) (2)
  24. HOBt (1)
  25. Imidazole (2)
  26. Isocyanate (2)
  27. Maleimide (1)
  28. Morpholine (2)
  29. NH2 (1)
  30. Piperazine (3)
  31. Piperidine (1)
  32. Potassium Permanganate (2)
  33. Propylsulfonic Acid (SCX-2) (8)
  34. Pyridine (2)
  35. Pyridinium Chlorochromate (PCC) (2)
  36. Pyridinium Dichromate (PDC) (2)
  37. S-Pd (1)
  38. SAX (1)
  39. SCX (2)
  40. SCX-2 (1)
  41. Silica (4)
  42. Silver Nitrate (AgNO3) (2)
  43. TAAcOH (5)
  44. TAAcONa (4)
  45. TBA Chloride (1)
  46. TBD (2)
  47. TEMPO (2)
  48. Thiol (5)
  49. Thiourea (4)
  50. TMA Acetate (5)
  51. TMA Chloride (SAX) (4)
  52. Tosic Acid (SCX) (8)
  53. Tosyl Chloride (2)
  54. Tosyl Hydrazine (2)
  55. Triamine (5)
  56. WAX (1)
  57. WCX (1)
Pore Size
  1. 60 Å (91)
  2. 25-70 Å (3)
Endcapping
  1. Endcapped (104)
  2. Non-endcapped (14)
Cartridges Volume
  1. 1 mL (18)
  2. 2 mL (1)
  3. 3 mL (22)
  4. 6 mL (23)
  5. 12 mL (23)
  6. 25 mL (23)
  7. 70 mL (6)
  8. 150 mL (6)
  9. 276 mL (6)
Bed Weight
  1. 50 mg (18)
  2. 100 mg (19)
  3. 200 mg (22)
  4. 500 mg (22)
  5. 1 g (23)
  6. 2 g (23)
  7. 4 g (15)
  8. 5 g (25)
  9. 8 g (2)
  10. 9 g (2)
  11. 10 g (6)
  12. 12 g (13)
  13. 15 g (6)
  14. 20 g (6)
  15. 25 g (19)
  16. 40 g (15)
  17. 45 g (2)
  18. 50 g (6)
  19. 70 g (6)
  20. 80 g (13)
  21. 90 g (4)
  22. 100 g (6)
  23. 120 g (13)
  24. 135 g (2)
  25. 200 g (2)
  26. 220 g (13)
  27. 330 g (13)
  28. 350 g (2)
  29. 400 g (2)
  30. 800 g (2)
Particle Size
  1. 40-63 µm / 230-400 mesh (91)
  2. 63-250 µm / 60-230 mesh (3)

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