> Advanced Search    > Product Reference Tool

Follow SiliCycle on Facebook Follow SiliCycle on Twitter Follow SiliCycle on LinkedIn Watch our videos on Youtube

SiliaPrep™- SPE & Well Plates, Metal Scavengers

SiliaPrep™ Metal Scavengers are unique and they have significantly changed how chemists can prepare active pharmaceutical ingredients (APIs). Any synthetic pathway is now possible, even the ones using metal catalysts. Treatment with SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes (Pd, Pt, Rh, Ru, Ni, Sn, etc.) to single digit ppm. Ask for the SiliaPrep Metal Scavengers brochure for more information and experimental results about these products.

Typical Experimental Procedure

To find out which SiliaPrep Metal Scavenger will better suit your need, we recommend performing some screening using the SiliaPrep Metal Scavenger Kit (PN: SPE-K30730B-06U) to quickly determine which scavenger presents the highest efficiency and make experiment optimization from there.

  1. SiliaPrep Metal Scavenger sorbent bed weight: use at least 4-8 eq. of the metal scavenger in respect to the residual metal concentration.
  2. Column conditioning using one column volume of methanol (or appropriate solvent).
  3. Sample application: add the metal containing solution to the top of the and let it pass through the SiliaPrep SPE under gravity.
  4. Washing the SiliaPrep SPE with additional solution solvent for total recovery of the API.
  5. Selection of the most efficient SiliaPrep Metal Scavenger by residual metal concentration analysis of each solution (the one with the lowest residual metal concentration). You can choose more than one scavenger.
  6. Experiment optimization using the most efficient SiliaPrep Metal Scavenger (modify the number of molar equivalents of the metal scavenger, change the reaction time (flow rate adjustment).

10 Item(s)

Set Descending Direction
per page

List  Grid 

  1. SiliaPrep™ SPE Cartridges Amine (WAX)

    SiliaPrep™ SPE Cartridges Amine (WAX)

    SiliaPrep Amine is a weak anion exchanger sorbent used in replacement of SAX for strong anions to avoid irreversible retention. Can also be employed as a metal scavenger and in normal phase conditions.

  2. SiliaPrep™ SPE Cartridges Amine nec (WAX)

    SiliaPrep™ SPE Cartridges Amine nec (WAX)

    SiliaPrep Amine nec is a weak anion exchanger sorbent used in replacement of SAX for strong anions to avoid irreversible retention. Can also be employed as a metal scavenger and norman phase conditions.

  3. SiliaPrep™ SPE Cartridges Diamine

    SiliaPrep™ SPE Cartridges Diamine

    SiliaPrep Diamine can be used in replacement of SAX for strong anions. It can also be employed as metal scavenger and in normal phase conditions.

  4. SiliaPrep™ SPE Cartridges Diamine nec

    SiliaPrep™ SPE Cartridges Diamine nec

    SiliaPrep diamine can be used in replacement of SAX for strong anions to be irreversible retention. Can also be employed as metal scavenger and in normal-phase conditions.

  5. SiliaPrep™ SPE Cartridges Triamine

    SiliaPrep™ SPE Cartridges Triamine

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  6. SiliaPrep™ SPE Cartridges Thiol

    SiliaPrep™ SPE Cartridges Thiol

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  7. SiliaPrep™ SPE Cartridges Thiourea

    SiliaPrep™ SPE Cartridges Thiourea

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  8. SiliaPrep™ SPE Cartridges TAAcOH

    SiliaPrep™ SPE Cartridges TAAcOH

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

  9. SiliaPrep™ SPE Cartridges TAAcONa

    SiliaPrep™ SPE Cartridges TAAcONa

    SiliaPrep Metal Scavengers will lower the residual metal concentration of variois metal complexes to single digit ppm.

  10. SiliaPrep™ SPE Cartridges Dimercaptotriazine (DMT)

    SiliaPrep™ SPE Cartridges Dimercaptotriazine (DMT)

    SiliaPrep Metal Scavengers will lower the residual metal concentration of various metal complexes to single digit ppm.

10 Item(s)

Set Descending Direction
per page

List  Grid 

Filter By
Metal to Remove
Silver (Ag)
  1. Preferred Scavengers (1)
  2. Scavenge (1)
Calcium (Ca)
  1. Preferred Scavengers (1)
Cadmium (Cd)
  1. Preferred Scavengers (3)
  2. Scavenge (3)
Cobalt (Co)
  1. Preferred Scavengers (1)
  2. Scavenge (6)
Chromium (Cr)
  1. Preferred Scavengers (5)
  2. Scavenge (2)
Cesium (Cs)
  1. Preferred Scavengers (1)
  2. Scavenge (1)
Copper (Cu)
  1. Preferred Scavengers (1)
  2. Scavenge (8)
Iron (Fe)
  1. Preferred Scavengers (1)
  2. Scavenge (8)
Mercury (Hg)
  1. Preferred Scavengers (1)
  2. Scavenge (4)
Iridium (Ir)
  1. Preferred Scavengers (2)
  2. Scavenge (1)
Lanthanum (La)
  1. Preferred Scavengers (1)
Lithium (Li)
  1. Preferred Scavengers (1)
Magnesium (Mg)
  1. Preferred Scavengers (1)
Nickel (Ni)
  1. Preferred Scavengers (2)
  2. Scavenge (4)
Osmium (Os)
  1. Preferred Scavengers (3)
  2. Scavenge (2)
Lead (Pb)
  1. Preferred Scavengers (1)
  2. Scavenge (5)
Palladium (Pd-2+)
  1. Preferred Scavengers (6)
  2. Scavenge (4)
Palladium (Pd-0)
  1. Preferred Scavengers (6)
  2. Scavenge (2)
Platinum (Pt)
  1. Preferred Scavengers (6)
Rhodium (Rh-1+)
  1. Preferred Scavengers (3)
  2. Scavenge (4)
Rhodium (Rh-2+)
  1. Preferred Scavengers (3)
  2. Scavenge (4)
Rhodium (Rh-3+)
  1. Preferred Scavengers (2)
  2. Scavenge (2)
Ruthenium (Ru-2+)
  1. Preferred Scavengers (1)
  2. Scavenge (5)
Scandium (Sc)
  1. Preferred Scavengers (2)
  2. Scavenge (3)
Tin (Sn)
  1. Preferred Scavengers (1)
  2. Scavenge (3)
Tungsten (W)
  1. Scavenge (5)
Zinc (Zn)
  1. Scavenge (7)
Family / Formats
  1. SiliaPrep™ (SPE Cartridges) (10)
Array
  1. Amine (2)
  2. Diamine (2)
  3. Dimercaptotriazine (DMT) (1)
  4. TAAcOH (1)
  5. TAAcONa (1)
  6. Thiol (1)
  7. Thiourea (1)
  8. Triamine (1)
Pore Size
  1. 60 Å (10)
Endcapping
  1. Endcapped (10)
  2. Non-endcapped (2)
Cartridges Volume
  1. 1 mL (5)
  2. 3 mL (9)
  3. 6 mL (10)
  4. 12 mL (10)
  5. 25 mL (10)
Bed Weight
  1. 50 mg (4)
  2. 100 mg (5)
  3. 200 mg (9)
  4. 500 mg (9)
  5. 1 g (10)
  6. 2 g (10)
  7. 5 g (10)
Particle Size
  1. 40 - 63 µm / 230 - 400 mesh (10)

Collapse All | Expend All

New E-PAK cartridges for large-scale purification processes
New SiliCycle Guide for Chemical Synthesis & Purification
Choose the right SiliCycle MiniBlock for your chemistry
Défi Cosmétique in silica(tm) - Initiative Cosmétique

Blog

Recent Posts

 
My Cart

You have no items in your shopping cart.

 
 
Compare Products

You have no items to compare.

 


© 2018 SiliCycle.

Follow us and get our news and promotions! Follow SiliCycle on Facebook Follow SiliCycle on Twitter Follow SiliCycle on LinkedIn Watch our videos on Youtube

Worldwide Headquarters SiliCycle Inc., 2500, Parc-Technologique Blvd, Quebec City (Quebec) G1P 4S6, CANADA
Phone: +1 418.874.0054 / Toll Free: +1 877.745.4292 (North America only)
Fax: +1 418.874.0355 E-mail: info@silicycle.com
Copyright © 2018 SiliCycle Inc. All rights reserved.