Follow SiliCycle on Facebook Follow SiliCycle on Twitter Follow SiliCycle on LinkedIn Watch our videos on Youtube

Triazoles

> back to Suggested SPE Protocols

Matrix

Plasma

Analytes

Fluconazole, Voriconazole, Posaconazole, Ketoconazole, Hydroxy-itraconazole, Itraconazole

SPE Cartridge

SiliaPrepX DVB
30 mg / 1 mL
SPE-P0001-01AA

Sample Pretreatment before Loading

Dilute 300 μL of plasma to 1 mL, adjust pH to 2.0.

Conditionning

1 mL of Methanol

Equilibration

1 mL of Water

Loading

Pretreated sample

Washing

1 mL of 1 % Ammonium Hydroxide in Water
1 mL of Water / Methanol (70:30)

Elution

1 mL of Methanol

Further Treatment

Evaporation under Nitrogen, reconstitution with Water / Methanol (50:50) and identification by HPLC.

1 Item(s)

Set Descending Direction
per page

List  Grid 

  1. SiliaPrepX DVB Polymeric SPE Cartridges, 85 µm, 60 Å (SPE-P0001)

    SiliaPrepX Polymeric SPE Cartridges, DVB, 85 µm, 60 Å (SPE-P0001)

    SiliaPrepX DVB is a polystyrene-divinylbenzene copolymer presenting a high hydrophobicity used as reversed-phase for extraction of neutral, acidic and basic compounds in viscous matrices.

1 Item(s)

Set Descending Direction
per page

List  Grid