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 APPLICATION NOTE 

Efficient Use of E-PAK Technology for the Removal of a Widely Used Suzuki Catalyst

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Among the most popular reactions in organic chemistry for carbon-carbon (C-C) bond formation, the Suzuki-Miyaura cross coupling reaction allows the production of various compounds for the pharmaceutical, chemical, drug, agrochemical, and polymer industries. With the new ICH-Q3D guidelines on concentration limits for the residues of metal catalysts, SiliCycle’s chemists compared the efficiency of various metal scavengers in removing traces of one of the most popular Suzuki catalyst, Pd(PPh3)4. All screenings were performed using the MiniBlock apparatus to determine which scavengers were the most successful in removing traces of leftover palladium-catalyst. The main objective was to demonstrate a direct and straightforward transfer to the E-PAK technology.

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Find below the list of our various E-PAK cartridges and housing:

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  1. Laboratory Scale SiliaMetS® Thiol E-PAK® Cartridges for metal purification
  2. Laboratory Scale SiliaMetS® Thiol E-PAK® Cartridges for metal purification
  3. Laboratory Scale C-941 Activated Carbon E-PAK® Cartridges for purification
  4. Laboratory Scale C-944 Activated Carbon E-PAK® Cartridges for purification
  5. Laboratory Scale C-947 Activated Carbon E-PAK® Cartridges for purification
  6. Laboratory Scale C-948 Activated Carbon E-PAK® Cartridges for purification
  7. Commercial Scale SiliaMetS E-PAK Cartridges, 16.5 x 100 cm

    Commercial Scale SiliaMetS E-PAK Cartridges, 16.5 x 100 cm

    E-PAK commercial scale cartridges with silica-based metal scavenger: SiliaMets Thiol or SiliaMetS DMT
  8. Commercial Scale Activated Carbon E-PAK Cartridges, 16.5 x 100 cm
  9. Commercial Scale SiliaMetS E-PAK Cartridges, 16.5 x 50 cm

    Commercial Scale SiliaMetS E-PAK Cartridges, 16.5 x 50 cm, 1/box

    E-PAK commercial scale cartridges with silica-based metal scavenger: SiliaMets Thiol or SiliaMetS DMT
  10. Commercial Scale Activated Carbon E-PAK Cartridges, 16.5 x 50 cm
  11. Pilot Scale SiliaMetS E-PAK Cartridges, 16.5 x 25 cm

    Pilot Scale SiliaMetS E-PAK Cartridges, 16.5 x 25 cm, 1/box

    E-PAK pilot scale cartridges with silica-based metal scavenger: SiliaMets Thiol or SiliaMetS DMT
  12. Pilot Scale Activated Carbon E-PAK Cartridges, 16.5 x 25 cm
  13. Pilot Scale SiliaMetS E-PAK Cartridges, 16.5 x 12.5 cm

    Pilot Scale SiliaMetS E-PAK Cartridges, 16.5 x 12.5 cm, 1/box

    E-PAK pilot scale cartridges with silica-based metal scavenger: SiliaMets Thiol or SiliaMetS DMT
  14. Pilot Scale Activated Carbon E-PAK Cartridges, 16.5 x 12.5 cm
  15. Laboratory Scale SiliaMetS Thiol E-PAK Cartridges, 5 x 10 cm
  16. Laboratory Scale SiliaMetS Thiol E-PAK 5 x 10cm cartridges for metal purification
  17. Laboratory Scale C-941 Activated Carbon E-PAK 5 x 10 cm Cartridges for purification
  18. Laboratory Scale C-944 Activated Carbon E-PAK 5 x 10 cm Cartridges for purification
  19. Laboratory Scale C-947 Activated Carbon E-PAK 5 x 10 cm Cartridges for purification
  20. Laboratory Scale C-948 Activated Carbon E-PAK 5 x 10 cm Cartridges for purification
  21. Laboratory Scale SiliaMetS Thiol E-PAK® 5 x 25 cm Cartridges for metal removal
  22. Laboratory Scale SiliaMetS Thiol E-PAK 5 x 25 cm cartridges for metal purification
  23. Laboratory Scale C-941 Activated Carbon E-PAK 5 x 25 com Cartridges for purification
  24. Laboratory Scale C-947 Activated Carbon E-PAK 5 x 25 com Cartridges for purification
  25. Laboratory Scale C-948 Activated Carbon E-PAK 5 x 25 com Cartridges for purification
  26. Housing for 16.5 x 12.5 cm E-PAK Cartridges, Single Round (PSHSR-12)
  27. Housing for 16.5 x 25 cm E-PAK Cartridges, Single Round (PSHSR-25)
  28. Housing for 16.5 x 50 & 100 cm E-PAK Cartridges, Single Round (CSHSR-50100)
  29. Bowl for Laboratory Scale E-PAK Housing, 5 x 1 cm (LS-BOWL1)
  30. Bowl for Laboratory Scale E-PAK Housing, 5 x 10 cm (LS-BOWL10)
  31. Bowl for Laboratory Scale E-PAK Housing, 5 x 25 cm
  32. Housing Kit for 5 x 1 cm Laboratory Scale E-PAK Cartridges (LSHK-1)
  33. Housing Kit for 5 x 10 cm Laboratory Scale E-PAK Cartridges (LSHK-10)
  34. Housing Kit for 5 x 25 cm Laboratory Scale E-PAK Cartridges (LSHK-25)
  35. Housing Kit for Laboratory Scale E-PAK Cartridges, with 2 bowls (LSHK-110)
  36. Housing Kit for Laboratory Scale E-PAK Cartridges, with 2 bowls (LSHK-125)
  37. Housing Kit for Laboratory Scale E-PAK Cartridges, with 3 bowls (LSHK-11025)

    Housing Kit for Laboratory Scale E-PAK Cartridges, with 3 bowls (LSHK-11025)

    Lab scale housing kit including 3 bowls: 5 x 1 ; 5 x 10 & 5 x 25 cm.
  38. E-PAK Cartridges, SiliaFlash Silica, 40 - 63 µm, 5 x 1 cm (LS-R10030B-1CM)
  39. E-PAK Cartridges, SiliaFlash Silica, 60 - 200 µm, 5 x 1 cm (LS-R10040B-1CM)
  40. E-PAK Cartridges, SiliaFlash Silica, 200 - 500 µm, 5 x 1 cm (LS-R10170B-1CM)
  41. E-PAK Cartridges, SiliaFlash Silica, 43 - 60 µm, 5 x 10 cm (LS-R10030B-10CM)
  42. E-PAK Cartridges, SiliaFlash Silica, 60 - 200 µm, 5 x 10 cm (LS-R10040B-10CM)
  43. E-PAK Cartridges, SiliaFlash Silica, 200 - 500 µm, 5 x 10 cm (LS-R10170B-10CM)
  44. E-PAK Cartridges, SiliaFlash Silica, 43 - 60 µm, 5 x 25 cm (LS-R10030B-25CM)
  45. E-PAK Cartridges, SiliaFlash Silica 60 - 200 µm, 5 x 25 cm (LS-R10040B-25CM)
  46. E-PAK Cartridges, SiliaFlash Silica 200 - 500 µm, 5 x 25 cm (LS-R10170B-25CM)

46 Item(s)

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