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SiliaBond Tosyl Hydrazine solid-phase extraction coupled online with HPLC-FLD for the quantification of zearalenone in edible oil

SiliaBond Tosyl Hydrazine solid-phase extraction coupled online with HPLC-FLD for the quantification of zearalenone in edible oil

SiliaBond Tosyl Hydrazine proved to be the best supported hydrazine material in the reversible covalent extraction of zearalenone.

Zearalenone (ZEN) is a mycotoxin found in edible oils which requires close monitoring to comply with established maximum levels. Sample preparation can be problematic, hence an in-line SPE-HPLC protocol was developped involving a reversible hydrazone

Keywords:
Zearalenone, Covalent SPE, in-line SPE-HPLC, edible oil

> SiliaBond Tosyl Hydrazine

> SiliaBond Functionalized Silica Gels

 

Publication Automated solid-phase extraction coupled online with HPLC-FLD for the quantification of zearalenone in edible oil
Authors Sarah S. Drzymala, Stefan Weiz, Julia Heinze, Silvia Marten, Carsten Prinz, Annett Zimathies, Leif-Alexander Garbe and Matthias Koch
Organization Department of Analytical Chemistry, Reference Materials, Federal Institute for Materials Research and Testing (BAM), Richard-Willstätter-Str. 11, 12489, Berlin (Germany)
Source Analytical and Bioanalytical Chemistry, May 2015, Volume 407, Issue 12, pp 3489-3497
Date 2015
Reaction scheme Reaction Scheme of SiliaBond Tosyl Hydrazine solid-phase extraction online coupling with HPLC-FLD for the quantification of zearalenone in edible oil
Full publication http://link.springer.com/article/10.1007/s00216-015-8541-5

 

SiliaBond Functionalized Silica Gels

SiliaBond Functionalized Silica Gels

SiliCycle is the leader in the development of functionalized silica gels, gathered under the name SiliaBond, for use in organic synthesis. The backbone of all SiliaBond products is SiliCycle SiliaFlash F60 which provides superior performance for all types of applications due to the narrow particle size distribution and high purity.

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SiliaBond Functionalized Silica Gels: